|
DDC
| 615 | |
Tác giả CN
| Đào, Thị Cẩm Minh | |
Nhan đề
| Xây dựng phương pháp phát hiện đồng thời một số thuốc giảm đau, kháng viêm trộn trái phép trong chế phẩm đông dược bằng LC-MS/MS / Đào Thị Cẩm Minh, Thái Khoa Bảo Châu, Trần Tuấn Phong, Nguyễn Phúc Khánh Nhi, Trần Hữu Dũng, Phạm Thị Thanh Hà, Nguyễn Thị Kiều Anh | |
Tóm tắt
| A liquid chromatography coupled with tandem-mass spectrometry (LC-MS/MS) method was developed for simultaneous determination of 9 analgesic and anti-inflammatory drugs, illegally added as adulterants to relevant herbal products. Blank matrix was based on the corresponding traditional remedy (Vietnamese Pharmacopoeia IV). Simple and rapid sample treatment was performed by methanol extraction. LC-MS/MS conditions were chosen for simultaneous determination of these 9 substances and optimized for relatively short retention time. The method was validated in accordance with AOAC 2016 and ICH 2005 guidelines. On practical application, 30 herbal products were analyzed. Of these five were detected as adulterated with paracetamol, indomethacin and dexamethasone acetate. | |
Thuật ngữ chủ đề
| Nghiên cứu - Kỹ Thuật --Việt Nam | |
Từ khóa tự do
| Kháng viêm | |
Từ khóa tự do
| LC-MS/MS | |
Tác giả(bs) CN
| Thái, Khoa Bảo Châu | |
Nguồn trích
| Tạp chí Dược học 2018tr. 18-22
Số: 03 |
| |
000
| 00000nab#a2200000ui#4500 |
|---|
| 001 | 18874 |
|---|
| 002 | 9 |
|---|
| 004 | 2EA4AF3A-CD5A-4916-8F5A-A1E17715CB24 |
|---|
| 005 | 201912121623 |
|---|
| 008 | 081223s vm| vie |
|---|
| 009 | 1 0 |
|---|
| 039 | |y20191212162309|zthienvan |
|---|
| 082 | |a615 |
|---|
| 100 | |aĐào, Thị Cẩm Minh |
|---|
| 245 | |aXây dựng phương pháp phát hiện đồng thời một số thuốc giảm đau, kháng viêm trộn trái phép trong chế phẩm đông dược bằng LC-MS/MS / |cĐào Thị Cẩm Minh, Thái Khoa Bảo Châu, Trần Tuấn Phong, Nguyễn Phúc Khánh Nhi, Trần Hữu Dũng, Phạm Thị Thanh Hà, Nguyễn Thị Kiều Anh |
|---|
| 520 | |aA liquid chromatography coupled with tandem-mass spectrometry (LC-MS/MS) method was developed for simultaneous determination of 9 analgesic and anti-inflammatory drugs, illegally added as adulterants to relevant herbal products. Blank matrix was based on the corresponding traditional remedy (Vietnamese Pharmacopoeia IV). Simple and rapid sample treatment was performed by methanol extraction. LC-MS/MS conditions were chosen for simultaneous determination of these 9 substances and optimized for relatively short retention time. The method was validated in accordance with AOAC 2016 and ICH 2005 guidelines. On practical application, 30 herbal products were analyzed. Of these five were detected as adulterated with paracetamol, indomethacin and dexamethasone acetate. |
|---|
| 650 | |aNghiên cứu - Kỹ Thuật |zViệt Nam |
|---|
| 653 | |aKháng viêm |
|---|
| 653 | |aLC-MS/MS |
|---|
| 700 | |aThái, Khoa Bảo Châu |
|---|
| 773 | |tTạp chí Dược học |d2018|gtr. 18-22|i03 |
|---|
| 890 | |c1|a0|b0|d4 |
|---|
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